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ผลงานตีพิมพ์ในวารสารวิชาการDetermination of phase ratio in polymorphic materials by x-ray absorption spectroscopy: The case of anatase and rutile phase mixture in TiO2ผู้แต่ง:Smith, M.F, Klysubun, W, Kityakarn, S, Dr.Attera Worayingyong, Associate Professor, Zhang, S.B, Wei, S.-H, Onkaw, D, Songsiriritthigul, P, Rujirawat, S, Limpijumnong, S, วารสาร: |
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หัวเรื่อง:ไม่มีชื่อไทย (ชื่ออังกฤษ : Phase Characterization of TiO2 Powder by XRD and TEM) ผู้เขียน:เขมฤทัย ถามะพัฒน์ สื่อสิ่งพิมพ์:pdf AbstractIn this study, the commercial TiO2 nanopowder and micropowder of anatase phase and rutile phase have been characterized by x-ray diffraction (XRD) and transmission electron microscopy (TEM). XRD patterns of nano-TiO2 in rutile and anatase phases exhibit broad peaks whereas both phases of micro-TiO2 demonstrate very sharp peaks. TEM images show that the grain size of TiO2 micropowders and TiO2 nanopowders are 0.3-0.7 ?m and 10 nm, respectively. The selected-area electron diffraction patterns of TiO2 nanopowders in rutile and anatase phases are consistent with XRD results. |
หัวเรื่อง:ไม่มีชื่อไทย (ชื่ออังกฤษ : Structures and Optical Properties of TiO2 Thin Films Deposited on Unheated Substrate by DC Reactive Magnetron Sputtering) ผู้เขียน:Nirun Witit-anun, Prasertsak Kasemanankul, Surasing Chaiyakun, พิเชษฐ ลิ้มสุวรรณ สื่อสิ่งพิมพ์:pdf AbstractTitanium dioxide thin films (TiO2) were deposited on unheated substrate on a glass slide and Si-wafer by the DC reactive magnetron sputtering method at different total pressures. The crystal structure, surface morphology and optical transmittance were characterized by X-ray diffractometer, atomic force microscopy and UV-VIS-NIR spectrophotometer, respectively. The deposited films were transparent and the thickness was about 133-168 nm. XRD results showed that all samples possessed a polycrystalline structure and changed from the mixed phase of anatase and rutile, to rutile phases, as the total pressure decreased. An increase in the film’s roughness was observed with increasing sputtering pressure. The optical transmission measurements revealed that the mixed phases of anatase and rutile had higher transmittance than the pure rutile phase. The refractive index, in the visible spectrum was relatively high, while the energy band gap was found to be 3.25 eV. |
ที่มา:การประชุมทางวิชาการของมหาวิทยาลัยเกษตรศาสตร์ ครั้งที่ 47หัวเรื่อง:โปรแกรมฝึกสอนคีย์บอร์ดเบื้องต้น |
หัวเรื่อง:ไม่มีชื่อไทย (ชื่ออังกฤษ : Structures and Optical Properties of TiO2 Thin Films Deposited on Unheated Substrate by DC Reactive Magnetron Sputtering) ผู้เขียน:Nirun Witit-anun, Prasertsak Kasemanankul, Surasing Chaiyakun, พิเชษฐ ลิ้มสุวรรณ สื่อสิ่งพิมพ์:pdf AbstractTitanium dioxide thin films (TiO2) were deposited on unheated substrate on a glass slide and Si-wafer by the DC reactive magnetron sputtering method at different total pressures. The crystal structure, surface morphology and optical transmittance were characterized by X-ray diffractometer, atomic force microscopy and UV-VIS-NIR spectrophotometer, respectively. The deposited films were transparent and the thickness was about 133-168 nm. XRD results showed that all samples possessed a polycrystalline structure and changed from the mixed phase of anatase and rutile, to rutile phases, as the total pressure decreased. An increase in the film’s roughness was observed with increasing sputtering pressure. The optical transmission measurements revealed that the mixed phases of anatase and rutile had higher transmittance than the pure rutile phase. The refractive index, in the visible spectrum was relatively high, while the energy band gap was found to be 3.25 eV. |
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